Nchịkọta ọrụ
A na-eji igbe mkpuchi aka maka ọrụ ụlọ nyocha batrị ebe achọrọ ikuku oxygen na mmiri dị ala. Enwere ike ịhazi ọnụ ụlọ ọrụ maka njikwa electrolyte, nkwadebe electrode, mgbakọ cell, akara na n'ime-nnwale ọnọdụ.
Ụlọ isi na-enye ikuku na-achịkwa. A na-eji nnukwu ụlọ na obere antechamber na-ebufe ihe na ngwá ọrụ na-enweghị imeghe ụlọ ọrụ na-arụ ọrụ na gburugburu ebe obibi.
Enwere ike iji nitrogen ma ọ bụ argon mee ihe dị ka gas na-arụ ọrụ. Emebere usoro nchacha na mgbasa ozi iji kwado mmiri na ikuku oxygen n'okpuru 1 ppm n'okpuru ọnọdụ nnabata akọwapụtara.
Enwere ike ịkwado ụlọ ahụ na ntinye ntinye ọzọ, njikọ oghere, ngwa ọkụ na ngwa ndị ọzọ dabere na usoro ụlọ nyocha.
Nhazi igbe mkpuchi
Ime ụlọ na-arụ ọrụ bụ nke igwe anaghị agba nchara 304 nwere windo ihu 8 mm chọrọ maka nlele anya nke mpaghara ọrụ. Ụlọ ahụ na-agụnye shelf igwe anaghị agba nchara atọ na ọkụ agbakwunyere.
Ọdụ ụgbọ mmiri na-eji ihe aluminom alloy nwere akara akara O{0}. A na-enye gloves butyl maka ịrụ ọrụ n'ime ụlọ.
Enyere ọdụ ụgbọ mmiri DN 40 KF asaa na otu ike 220 V maka ijikọ akụrụngwa inyeaka. Enwere ike ịhazi oghere ndị ọzọ mgbe achọrọ ya.
Sistemụ Antechamber
A na-eji igbe uwe aka nwere ma nnukwu antechamber na obere ụlọ maka ịnyefe ihe n'etiti ebe dịpụrụ adịpụ na ikuku na-achịkwa.
Nnukwu antechamber nwere dayameta nke 360 mm na ogologo 600 mm. Ọ gụnyere igwe anaghị agba nchara sliding tray, ụzọ abụọ na ihe nrụgide. A na-achịkwa mgbapụta Vacuum na ntinye gas site na sistemụ mmetụ aka.
Obere ụlọ antechamber nwere dayameta nke 150 mm na ogologo 300 mm. Ọ na-eji valvụ aka wee na-atụgharị-bọtịnụ ụzọ ọrụ ma e bu n'obi mee ya maka obere sample na ngwaọrụ.
Ọcha gas na okirikiri
Usoro nchacha ahụ na-eji ihe na-eme ka ọla kọpa na sieve molecular wepụ oxygen na mmiri na ikuku na-arụ ọrụ.
Ihe eji eme ka ọ dị ọcha na-agụnye 5 n'arọ nke ihe na-akpata ọla kọpa na 5 n'arọ nke sieve molecular. Ikike ịdị ọcha akọwapụtara bụ 60 L maka iwepụ oxygen na 2 n'arọ maka iwepụ mmiri.
Enwere ike iji nitrogen ma ọ bụ argon mee ihe dị ka gas na-arụ ọrụ. Igwe na-ekesa mgbasa ozi agbakwunyere na-enye ọsọ ọsọ nke ihe dịka 90 m³ / h.
N'oge mmeghari ohuru, PLC na-achịkwa usoro ntughari na-akpaghị aka. Gas na-emegharị ahụ bụ ngwakọta nke gas na-arụ ọrụ na hydrogen, yana ntinye hydrogen nke 5-10%.
Nrụgide na njikwa ikuku
Usoro nchịkwa na-enye ohere ka arụ ọrụ nke igbe aka na antechambers gbanwee n'ime ± 10 mbar. A na-arụ ọrụ njikwa nchekwa mgbe nrụgide karịrị oke arụ ọrụ akọwapụtara.
Sistemu nwere ike ịrụ mgbapụta ikuku na-akpaghị aka na ntinye gas maka nnukwu ụlọ ante. Otu - ihicha ikuku dịkwa maka iji dochie ikuku dị n'ime ụlọ ọrụ.
Enwere ike ịtọ ụkpụrụ ikuku oxygen na mmiri dị ka usoro chọrọ. Mgbe uru ọ bụla gafere oke edobere, sistemụ na-enye mkpu.
PLC na-edekọ data arụ ọrụ dị ka ọkwa oxygen, ọkwa mmiri na ọkwa sistemụ. Enwere ike ịlele ndekọ akụkọ ihe mere eme site na ihuenyo mmetụ aka.
Sistemụ Vacuum na nlekota oru
Sistemụ agụụ na-eji Edwards rotary vane vacuum mgbapụta nwere ọnụego erute nke 12m³/h. Enwere ike iji aka ma ọ bụ chịkwaa mgbapụta ahụ site na PLC.
A na-eji usoro oghere maka ịpụpụ ụlọ antechamber na idobe ọnọdụ nrụgide achọrọ n'oge nnyefe ihe.
Ihe mmetụta ikuku oxygen nwere oke nha nke 0–1000 ppm, yana njiri mara nke 0.2 ppm. Ihe mmetụta mmiri ahụ nwekwara oke nha nke 0–1000 ppm ma dabara adaba maka ngwa gụnyere nyocha batrị na igwe- njikwa ihe akụrụngwa.
Enwere ike itinye ihe mgbasa ozi ihe mgbaze organic n'ime ụlọ. Nhazi ọkọlọtọ na-eji 10 n'arọ nke sieve molecular maka mgbasa ozi mgbaze na mmụgharị.
A na-etinye ihe mkpuchi ikuku nke ụlọ ọrụ n'elu igbe uwe aka. Ikike jụrụ oyi bụ 1050 W, yana mgbanwe mgbanwe okpomọkụ nke ogo 15-36.
Ngwa ngwa
Ụlọ ọrụ mmekọ
Ajụjụ a na-ajụkarị
Kedu ihe a na-eji igbe mkpuchi aka?
A na-eji igbe aka maka nyocha batrị, nkwadebe electrode, mgbakọ cell, njikwa electrolyte na usoro ndị ọzọ na-achọ ikuku oxygen na ọkwa mmiri.
Kedu gas nwere ike iji na igbe mkpuchi?
Usoro na-akwado nitrogen ma ọ bụ argon dị ka gas na-arụ ọrụ. Nhọrọ gas na-adabere na ihe batrị na ụlọ nyocha chọrọ.
Kedu ọkwa ikuku oxygen na mmiri nwere ike nweta igbe mkpuchi?
N'okpuru ọnọdụ ọkọlọtọ akọwapụtara, enwere ike idowe ọkwa mmiri na oxygen n'okpuru 1 ppm.
Enwere ike ịhazi igbe uwe aka?
Ee. Enwere ike ịhazi nhazi ụlọ, ụlọ antechamber, sistemu ịsacha ọcha, sistemu agụụ, ihe ọkụ eletrik na ngwa ndị ọzọ dịka ihe ndị ahịa chọrọ.
Enwere ike itinye akụrụngwa ụlọ nyocha ọzọ n'ime igbe uwe aka?
Ee. Nhazi modular na-enye ohere ka akụrụngwa na ngwa ndị ahọpụtara, dị ka efere kpo oku, akpịrịkpa, njikọ oghere na ntinye ọkụ eletrik, ka ejikọta ya na ngwa ahụ.
Kedu ihe dị iche n'etiti nnukwu na obere ụlọ antechamber?
Nnukwu antechamber dị mma maka ịnyefe ihe ndị buru ibu ma ọ bụ ihe onwunwe, ebe a na-ezubere obere ụlọ maka obere ihe na ịnyefe ihe eji eme ihe.
Igbe uwe aka adabara maka nrụpụta batrị lithium?
Ee. Sistemu dabara adaba maka batrị lithium R&D, nkwadebe electrode, mgbakọ cell, njikwa elektrọt na pilot{1}} nrụpụta batrị n'ụba.
Kedu ozi achọrọ maka igbe aka ahaziri ahazi?
Ndị ahịa nwere ike ịnye nha ọnụ ụlọ achọrọ, ụdị batrị, gas na-arụ ọrụ, ikuku oxygen na iru mmiri, nyefe chọrọ ụlọ na ihe ndị ọzọ chọrọ akụrụngwa. SZO nwere ike ịkwado nhazi kwesịrị ekwesị.